{"id":1406,"date":"2020-10-18T14:56:06","date_gmt":"2020-10-18T05:56:06","guid":{"rendered":"https:\/\/hatsudy.com\/jp\/?p=1406"},"modified":"2022-03-06T22:18:31","modified_gmt":"2022-03-06T13:18:31","slug":"wittig","status":"publish","type":"post","link":"https:\/\/hatsudy.com\/jp\/wittig.html","title":{"rendered":"Wittig\u53cd\u5fdc\uff1a\u30ab\u30eb\u30dc\u30cb\u30eb\u5316\u5408\u7269\u3068\u30ea\u30f3\u30a4\u30ea\u30c9\u304b\u3089\u30a2\u30eb\u30b1\u30f3\u3092\u5408\u6210\u3059\u308b"},"content":{"rendered":"<p>\u5206\u5b50\u306b\u70ad\u7d20\u9396\u3092\u5c0e\u5165\u3059\u308b\u3053\u3068\u306f\u3001\u6709\u6a5f\u5316\u5b66\u3067\u5316\u5408\u7269\u5408\u6210\u3092\u3059\u308b\u3068\u304d\u306b\u975e\u5e38\u306b\u91cd\u8981\u3067\u3059\u3002\u3053\u3046\u3057\u305f\u5408\u6210\u53cd\u5fdc\u306e\u4e00\u3064\u306bWittig\u53cd\u5fdc\uff08\u30a6\u30a3\u30c3\u30c6\u30a3\u30d2\u53cd\u5fdc\uff09\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n<p>Wittig\u53cd\u5fdc\u3067\u306f\u3001\u30ab\u30eb\u30dc\u30cb\u30eb\u57fa\uff08\u30b1\u30c8\u30f3\uff09\u307e\u305f\u306f\u30db\u30eb\u30df\u30eb\u57fa\uff08\u30a2\u30eb\u30c7\u30d2\u30c9\uff09\u3092\u30a2\u30eb\u30b1\u30f3\u306b\u5909\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002\u3064\u307e\u308a<span 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loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-1523\" src=\"https:\/\/hatsudy.com\/jp\/wp-content\/uploads\/2020\/10\/wrhf5-1.jpg\" alt=\"\" width=\"600\" height=\"134\" \/><\/p>\n<p>\u30ea\u30f3\u30a4\u30ea\u30c9\u304c\u6c42\u6838\u653b\u6483\u3057\u305f\u5f8c\u3001\u30de\u30a4\u30ca\u30b9\u306e\u96fb\u8377\u3092\u6709\u3059\u308b\u9178\u7d20\u539f\u5b50\u306f\u30ea\u30f3\u539f\u5b50\u3092\u653b\u6483\u3057\u307e\u3059\u3002\u305d\u306e\u7d50\u679c\u3001\u56db\u54e1\u74b0\u306e\u4e2d\u9593\u4f53\u304c\u751f\u6210\u3055\u308c\u307e\u3059\u3002\u3053\u306e\u4e2d\u9593\u4f53\u3092\u30aa\u30ad\u30b5\u30db\u30b9\u30d5\u30a7\u30bf\u30f3\uff08oxaphosphetane\uff09\u3068\u3044\u3044\u307e\u3059\u3002<\/p>\n<p>\u30aa\u30ad\u30b5\u30db\u30b9\u30d5\u30a7\u30bf\u30f3\u4e2d\u9593\u4f53\u306f\u975e\u5e38\u306b\u4e0d\u5b89\u5b9a\u306a\u5316\u5408\u7269\u3067\u3059\u3002\u305d\u306e\u305f\u3081<span style=\"color: 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style=\"color: #ff0000;\">\u30ea\u30f3\u30a4\u30ea\u30c9\u306f\u5b89\u5b9a\u30a4\u30ea\u30c9\u3068\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u306e2\u7a2e\u985e\u304c\u5b58\u5728\u3057\u307e\u3059\u3002<\/span>\u5b89\u5b9a\u30a4\u30ea\u30c9\u3067\u306f\u3001\u305d\u306e\u540d\u306e\u901a\u308a\u5b89\u5b9a\u72b6\u614b\u306e\u30a4\u30ea\u30c9\u3067\u3059\u3002\u4e00\u65b9\u306e\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u3060\u3068\u3001\u4e0d\u5b89\u5b9a\u306a\u72b6\u614b\u3067\u5b58\u5728\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n<p>\u3069\u306e\u3088\u3046\u306a\u3068\u304d\u3001\u5b89\u5b9a\u30a4\u30ea\u30c9\u306b\u306a\u308b\u306e\u3067\u3057\u3087\u3046\u304b\u3002\u305d\u308c\u306f\u3001\u30de\u30a4\u30ca\u30b9\u306e\u96fb\u8377\u3092\u6709\u3059\u308b\u70ad\u7d20\u539f\u5b50\u306e\u96a3\u306b\u96fb\u5b50\u5438\u5f15\u57fa\u304c\u5b58\u5728\u3059\u308b\u3068\u304d\u3067\u3059\u3002\u96fb\u5b50\u5438\u5f15\u57fa\u3068\u3057\u3066\u306f\u3001\u4f8b\u3048\u3070\u4ee5\u4e0b\u306e\u5b98\u80fd\u57fa\u304c\u77e5\u3089\u308c\u3066\u3044\u307e\u3059\u3002<\/p>\n<ul>\n<li class=\"odd\">\u30cb\u30c8\u30ed\u57fa\uff08-NO<sub>2<\/sub>\uff09<\/li>\n<li class=\"odd\">\u30b7\u30a2\u30ce\u57fa\uff08-CN\uff09<\/li>\n<li class=\"even\">\u30ab\u30eb\u30dc\u30cb\u30eb\u57fa\uff08-CO\uff09<\/li>\n<li class=\"even\">\u30b9\u30eb\u30db\u30f3\u57fa\uff08\uff0dSO<sub>3<\/sub>H\uff09<\/li>\n<\/ul>\n<p>\u306a\u305c\u3001\u3053\u308c\u3089\u306e\u5b98\u80fd\u57fa\u304c\u5b58\u5728\u3059\u308b\u3068\u5b89\u5b9a\u30a4\u30ea\u30c9\u306b\u306a\u308b\u306e\u3067\u3057\u3087\u3046\u304b\u3002\u305d\u308c\u306f\u3001\u4ee5\u4e0b\u306e\u3088\u3046\u306a\u5171\u9cf4\u69cb\u9020\u5f0f\u3092\u66f8\u3051\u308b\u304b\u3089\u3067\u3059\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-1525\" src=\"https:\/\/hatsudy.com\/jp\/wp-content\/uploads\/2020\/10\/wrhf7.jpg\" alt=\"\" width=\"500\" height=\"116\" \/><\/p>\n<p>\u5b89\u5b9a\u30a4\u30ea\u30c9\u306f\u5358\u96e2\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<span style=\"color: #0000ff;\">\u96fb\u5b50\u5438\u5f15\u57fa\u304c\u5b58\u5728\u3059\u308b\u3053\u3068\u3067\u3001\u975e\u5e38\u306b\u5b89\u5b9a\u306a\u72b6\u614b\u306e\u5316\u5408\u7269\u3068\u3057\u3066Wittig\u8a66\u85ac\u3092\u4f5c\u308c\u307e\u3059\u3002<\/span><\/p>\n<p>\u4e00\u65b9\u306e\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u3067\u306f\u3001\u5b89\u5b9a\u30a4\u30ea\u30c9\u306e\u3088\u3046\u306a\u96fb\u5b50\u5438\u5f15\u57fa\u304c\u5b58\u5728\u3057\u307e\u305b\u3093\u3002\u3053\u306e\u5834\u5408\u306f\u6c34\u3084\u7a7a\u6c17\u3068\u89e6\u308c\u308b\u3053\u3068\u3067\u5206\u89e3\u3059\u308b\u305f\u3081\u3001\u5358\u96e2\u3059\u308b\u306e\u306f\u4e0d\u53ef\u80fd\u3067\u3059\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-1526\" src=\"https:\/\/hatsudy.com\/jp\/wp-content\/uploads\/2020\/10\/wrhf8.jpg\" alt=\"\" width=\"400\" height=\"137\" \/><\/p>\n<p>\u5b89\u5b9a\u30a4\u30ea\u30c9\u306f\u5358\u96e2\u53ef\u80fd\u3067\u3042\u308b\u3053\u3068\u304b\u3089\u3001\u30a4\u30ea\u30c9\u3068\u3057\u3066\u306f\u53cd\u5fdc\u6027\u304c\u60aa\u3044\u3067\u3059\u3002\u305d\u308c\u306b\u5bfe\u3057\u3066\u3001\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u306f\u5358\u96e2\u3067\u304d\u306a\u3044\u3082\u306e\u306e\u3001\u30a4\u30ea\u30c9\u3068\u3057\u3066\u306e\u53cd\u5fdc\u6027\u306f\u512a\u308c\u3066\u3044\u307e\u3059\u3002\u3044\u305a\u308c\u306b\u3057\u3066\u3082\u3001\u3053\u306e\u3088\u3046\u306b\u5b89\u5b9a\u30a4\u30ea\u30c9\u3068\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u304c\u5b58\u5728\u3059\u308b\u3053\u3068\u3092\u7406\u89e3\u3057\u307e\u3057\u3087\u3046\u3002<\/p>\n<h3>\u30b7\u30b9\u30fb\u30c8\u30e9\u30f3\u30b9\uff08EZ\u5316\u5408\u7269\uff09\u306e\u7acb\u4f53\u5316\u5b66\u5236\u5fa1\u304c\u53ef\u80fd<\/h3>\n<p>\u305d\u308c\u3067\u306f\u3001\u306a\u305c\u5b89\u5b9a\u30a4\u30ea\u30c9\u3068\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u3092\u7406\u89e3\u3059\u308b\u3053\u3068\u304c\u91cd\u8981\u306a\u306e\u3067\u3057\u3087\u3046\u304b\u3002\u305d\u308c\u306f\u3001\u7acb\u4f53\u5316\u5b66\u306e\u5236\u5fa1\u304c\u53ef\u80fd\u3060\u304b\u3089\u3067\u3059\u3002<\/p>\n<p>\u30a2\u30eb\u30b1\u30f3\u3092\u5408\u6210\u3059\u308b\u3068\u304d\u3001\u5fc5\u305a\u554f\u984c\u306b\u306a\u308b\u306e\u304b\u5e7e\u4f55\u7570\u6027\u4f53\u3067\u3059\u3002\u30b7\u30b9\u30fb\u30c8\u30e9\u30f3\u30b9\u306e\u554f\u984c\u304c\u751f\u3058\u308b\u306e\u3067\u3059\u3002\u305d\u3053\u3067EZ\u7570\u6027\u4f53\u306e\u3046\u3061\u3001E\u4f53\u307e\u305f\u306fZ\u4f53\u306e\u3069\u3061\u3089\u304b\u3092\u9078\u629e\u7684\u306b\u5f97\u3089\u308c\u308b\u3088\u3046\u306b\u5408\u6210\u3057\u306a\u3051\u308c\u3070\u3044\u3051\u307e\u305b\u3093\u3002<\/p>\n<p>Wittig\u53cd\u5fdc\uff08\u30a6\u30a3\u30c3\u30c6\u30a3\u30d2\u53cd\u5fdc\uff09\u3067\u306f\u3001<span style=\"color: #0000ff;\">\u5229\u7528\u3059\u308b\u30db\u30b9\u30db\u30cb\u30a6\u30e0\u30a4\u30ea\u30c9\u304c\u5b89\u5b9a\u30a4\u30ea\u30c9\u306a\u306e\u304b\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\u306a\u306e\u304b\u306b\u3088\u3063\u3066\u3001\u5408\u6210\u3055\u308c\u308b\u5316\u5408\u7269\u304cE\u4f53\u306a\u306e\u304bZ\u4f53\u306a\u306e\u304b\u304c\u5909\u308f\u308a\u307e\u3059\u3002<\/span>\u5177\u4f53\u7684\u306b\u306f\u3001Wittig\u8a66\u85ac\u306b\u3088\u3063\u3066\u4ee5\u4e0b\u306e\u9055\u3044\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n<ul>\n<li>\u5b89\u5b9a\u30a4\u30ea\u30c9\uff1a\u751f\u6210\u5316\u5408\u7269\u306fE\u4f53\uff08\u30c8\u30e9\u30f3\u30b9\uff09<\/li>\n<li>\u4e0d\u5b89\u5b9a\u30a4\u30ea\u30c9\uff1a\u751f\u6210\u5316\u5408\u7269\u306fZ\u4f53\uff08\u30b7\u30b9\uff09<\/li>\n<\/ul>\n<p>\u4e00\u822c\u7684\u306a\u30a2\u30eb\u30b1\u30f3\u751f\u6210\u3067\u306f\u3001EZ\u7570\u6027\u4f53\u3092\u660e\u78ba\u306b\u533a\u5225\u3057\u3066\u5408\u6210\u3059\u308b\u306e\u304c\u56f0\u96e3\u3067\u3059\u3002\u305d\u308c\u306b\u5bfe\u3057\u3066Wittig\u53cd\u5fdc\u3067\u306f\u3001\u3053\u308c\u3089\u3092\u533a\u5225\u3057\u3066\u5408\u6210\u3067\u304d\u307e\u3059\u3002<\/p>\n<h3>EZ\u7570\u6027\u4f53\u3092\u533a\u5225\u3057\u3066\u5408\u6210\u3067\u304d\u308b\u7406\u7531<\/h3>\n<p>\u306a\u305c\u3001\u30a4\u30ea\u30c9\u306e\u5b89\u5b9a\u6027\u306b\u3088\u3063\u3066EZ\u7570\u6027\u4f53\u306e\u5408\u6210\u3092\u5206\u3051\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u306e\u3067\u3057\u3087\u3046\u304b\u3002\u3053\u306e\u7406\u7531\u306b\u3064\u3044\u3066\u306f\u3001\u7acb\u4f53\u969c\u5bb3\u3084\u53ef\u9006\u53cd\u5fdc\u306e\u9055\u3044\u306b\u306a\u3069\u306b\u3088\u3063\u3066\u8aac\u660e\u3055\u308c\u3066\u3044\u307e\u3059\u3002<\/p>\n<p>\u5b89\u5b9a\u30a4\u30ea\u30c9\u3067\u306f\u3001\u30ea\u30f3\u539f\u5b50\u304c\u30ab\u30eb\u30dc\u30cb\u30eb\u70ad\u7d20\u3092\u653b\u6483\u3057\u3066\u30aa\u30ad\u30b5\u30db\u30b9\u30d5\u30a7\u30bf\u30f3\u3092\u5f62\u6210\u3059\u308b\u53cd\u5fdc\u304c\u53ef\u9006\u53cd\u5fdc\u3067\u3059\u3002\u305d\u306e\u305f\u3081<span style=\"color: #ff0000;\">\u4e2d\u9593\u4f53\u306e\u5b89\u5b9a\u6027\u3092\u8003\u3048\u305f\u3068\u304d\u3001\u30b7\u30b9\u4f53\uff08Z\u4f53\uff09\u3067\u306f\u7acb\u4f53\u969c\u5bb3\u304c\u8d77\u3053\u308a\u307e\u3059\u3002<\/span>\u30c8\u30e9\u30f3\u30b9\u4f53\uff08E\u4f53\uff09\u306e\u307b\u3046\u304c\u3001\u5927\u304d\u306a\u7f6e\u63db\u57fa\u304c\u53cd\u5bfe\u5074\u306b\u5b58\u5728\u3059\u308b\u305f\u3081\u3001\u5b89\u5b9a\u30a4\u30ea\u30c9\u3067\u306fE\u9078\u629e\u7684\u306b\u5408\u6210\u53cd\u5fdc\u304c\u9032\u884c\u3057\u307e\u3059\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-1531\" src=\"https:\/\/hatsudy.com\/jp\/wp-content\/uploads\/2020\/10\/eehrt2.jpg\" alt=\"\" width=\"500\" height=\"209\" 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